C₂₇H₄₁O₆PSi

Base Information

Chemical Name:C₂₇H₄₁O₆PSi
CAS No.:1269618-49-6
Molecular Formula:C₂₇H₄₁O₆PSi
Molecular Weight:520.678
Hs Code.:

C<sub>27</sub>H<sub>41</sub>O<sub>6</sub>PSi

Synonyms:C₂₇H₄₁O₆PSi

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Chemical Property of C₂₇H₄₁O₆PSi

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Technology Process of C₂₇H₄₁O₆PSi

There total 6 articles about C₂₇H₄₁O₆PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1378889-75-8
C₃₀H₄₃NO₃S₂Si

: 756-79-6
dimethyl methane phosphonate

: 1269618-49-6
C₂₇H₄₁O₆PSi

Guidance literature:: dimethyl methane phosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₃₀H₄₃NO₃S₂Si; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol301103d

Reference yield:

: 1140194-79-1
4-(tert-butyldiphenylsiloxy)butanal dimethyl acetal

: 1269618-49-6
C₂₇H₄₁O₆PSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2.25 h / -78 - 0 °C / Inert atmosphere

1.2: 4.5 h / -78 - -50 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

With n-butyllithium; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol301103d