benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

Base Information

Chemical Name:benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15
CAS No.:87530-88-9
Molecular Formula:C₃₅H₄₉NO₃
Molecular Weight:531.779
Hs Code.:

Synonyms:benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

Suppliers and Price of benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

There total 6 articles about benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 87530-87-8
C₄₂H₅₅NO₅S

: 87530-88-9
benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

Guidance literature:: With hydrogenchloride; In methanol; water; for 1.5h;
DOI:10.1016/S0040-4020(01)91938-6

Reference yield:

: 53639-76-2
(3β,5α,17β,22E)-ergosta-8,14,22-trien-3-ol benzoate

: 87530-88-9
benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

Guidance literature:: Multi-step reaction with 5 steps

1: 1.5 g / Jones reagent / diethyl ether; acetone; H₂O / 4 h

2: 64 percent / acetic acid, zinc / methanol / 6 h / Heating

3: 62 percent / pyridine, hydroxylamine hydrochloride / methanol / 1 h / Heating

4: 2.59 g / pyridine / 16 h

5: 65 percent / hydrochloric acid / methanol; H₂O / 1.5 h

With pyridine; hydrogenchloride; jones reagent; hydroxylamine hydrochloride; acetic acid; zinc; In methanol; diethyl ether; water; acetone;
DOI:10.1016/S0040-4020(01)91938-6

Reference yield:

: 36959-80-5
benzoate d'ergosterol B₃

: 87530-88-9
benzoate d'aza-14a D-homo ergostadiene-8(14),22 ol-3β one-15

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) perphtalic acid 2.) hydrochloric acid / 1.) ether, 0 deg C, 5h 30min 2.) methanol, reflux, 1h

2: 62 percent / pyridine, hydroxylamine hydrochloride / methanol / 1 h / Heating

3: 2.59 g / pyridine / 16 h

4: 65 percent / hydrochloric acid / methanol; H₂O / 1.5 h

With pyridine; hydrogenchloride; perphtalic acid; hydroxylamine hydrochloride; In methanol; water;
DOI:10.1016/S0040-4020(01)91938-6