(5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate

Base Information

Chemical Name:(5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate
CAS No.:1235982-58-7
Molecular Formula:C₂₆H₃₂O₄
Molecular Weight:408.538
Hs Code.:

Synonyms:(5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate

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Technology Process of (5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate

There total 1 articles about (5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1235982-56-5
7,7-dimethylnona-2,8-diynoic acid

: 1235982-57-6
(R)-5-((4-methoxybenzyloxy)methyl)hex-1-yn-3-ol

: 1235982-58-7
(5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate

Guidance literature:: 7,7-dimethylnona-2,8-diynoic acid; (R)-5-((4-methoxybenzyloxy)methyl)hex-1-yn-3-ol; With dmap; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo100867v

Reference yield: 90.0%

: 1235982-58-7
(5R)-6-(4-methoxybenzyloxy)-5-methylhex-1-yn-3-yl 7,7-dimethylnona-2,8-diynoate

: 1235982-59-8
2-((R)-3-(4-methoxybenzyloxy)-2-methylpropyl)-6,7,8,9-tetrahydro-6,6-dimethylnaphtho[2,1-c]furan-1(3H)-one

Guidance literature:: With chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II); In toluene; at 130 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jo100867v