Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp

Base Information

• Chemical Name: Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp
• CAS No.: 133343-29-0
• Molecular Formula: C₂₉H₃₃Cl₅N₄O₇
• Molecular Weight: 726.869
• Mol file: 133343-29-0.mol

Synonyms:Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp

Chemical Property of Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp

There total 2 articles about Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.4%

HCl-L-Pro-L-Aze-L-Pro-Opcp (133357-54-7) + (S)-1-(t-butoxycarbonyl)azetidine-2-carboxylic acid (51077-14-6) → Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp (133343-29-0)

Guidance literature:

With 4-methyl-morpholine; isobutyl chloroformate; In chloroform; -15 deg C to room temperature;

Reference yield:

Boc-L-Pro-L-Aze-L-Pro-Opcp (57705-79-0) → Boc-L-Aze-L-Pro-L-Aze-L-Pro-Opcp (133343-29-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / gaseous hydrogen chloride / dioxane / 0.5 h / 15 °C

2: 85.4 percent / isobutyl chloroformate, N-methylmorpholine / CHCl₃ / -15 deg C to room temperature

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In 1,4-dioxane; chloroform;

upstream raw materials:

HCl-L-Pro-L-Aze-L-Pro-Opcp

(S)-1-(t-butoxycarbonyl)azetidine-2-carboxylic acid

Boc-L-Pro-L-Aze-L-Pro-Opcp

Refernces