[(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc

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Chemical Name:[(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc
CAS No.:1394978-69-8
Molecular Formula:C₅₈H₄₀N₆OS₃Zn
Molecular Weight:998.583
Hs Code.:

Synonyms:[(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc

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Chemical Property of [(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc

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Technology Process of [(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc

There total 6 articles about [(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.7%

: [(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin

: 1394978-69-8
[(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc

Guidance literature:: With zinc diacetate; In methanol; chloroform; for 4h; Reflux;
DOI:10.1016/j.orgel.2011.12.014

Reference yield:

: 15155-41-6
4,7-dibromobenzo[c][1,2,5]thiadiazole

: 1394978-69-8
[(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / Reflux

2: trichlorophosphate / 1,2-dichloro-ethane / 12 h / 0 - 80 °C / Inert atmosphere

3: propionic acid / 2 h / 140 °C

4: trichlorophosphate / 1,2-dichloro-ethane / 12 h / 0 - 80 °C / Inert atmosphere

5: zinc diacetate / methanol; chloroform / 4 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc diacetate; trichlorophosphate; In methanol; chloroform; propionic acid; 1,2-dichloro-ethane; toluene; 1: Stille coupling / 2: Vilsmeier formylation / 4: Vilsmeier formylation;
DOI:10.1016/j.orgel.2011.12.014

Reference yield:

: 1201212-94-3
4,7-bis(4-methylthiophen-2-yl)benzo[1,2,5]thiadiazole

: 1394978-69-8
[(4-methylthiophen-5-formyl-2-yl)benzo[1,2,5]thiadiazol-4-yl]-4-methylthiophene-2-10,15,20-tris(4-methylphenyl)porphyrin zinc

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 12 h / 0 - 80 °C / Inert atmosphere

2: propionic acid / 2 h / 140 °C

3: trichlorophosphate / 1,2-dichloro-ethane / 12 h / 0 - 80 °C / Inert atmosphere

4: zinc diacetate / methanol; chloroform / 4 h / Reflux

With zinc diacetate; trichlorophosphate; In methanol; chloroform; propionic acid; 1,2-dichloro-ethane; 1: Vilsmeier formylation / 3: Vilsmeier formylation;
DOI:10.1016/j.orgel.2011.12.014