3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole

Base Information

Chemical Name:3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole
CAS No.:1392103-86-4
Molecular Formula:C₂₃H₁₆BrClN₂O
Molecular Weight:451.75
Hs Code.:

Synonyms:3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole

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Chemical Property of 3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole

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Technology Process of 3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole

There total 4 articles about 3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₂₃H₁₅BrClNO

: 1392103-86-4
3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; Reflux;

Reference yield:

: 57845-08-6
p-chloroacetophenone phenylhydrazone

: 1392103-86-4
3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole

Guidance literature:: Multi-step reaction with 4 steps

1.1: polyphosphoric acid / 0.25 h / 100 - 120 °C

2.1: trichlorophosphate / 0.5 h / 0 °C

2.2: 4.5 h / 0 - 40 °C

3.1: piperidine / ethylene glycol / 4 h / Reflux

4.1: hydroxylamine hydrochloride; sodium hydroxide / ethanol / Reflux

With piperidine; hydroxylamine hydrochloride; sodium hydroxide; trichlorophosphate; In ethanol; ethylene glycol;

Reference yield:

: 1217-83-0
2-(4-chlorophenyl)-1H-indole-3-carbaldehyde

: 1392103-86-4
3-[3-(4-bromophenyl)-4,5-dihydroisoxazol-5-yl]-2-(4-chlorophenyl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethylene glycol / 4 h / Reflux

2: hydroxylamine hydrochloride; sodium hydroxide / ethanol / Reflux

With piperidine; hydroxylamine hydrochloride; sodium hydroxide; In ethanol; ethylene glycol;