1-butyl-4-deuteriobenzene

Base Information

• Chemical Name: 1-butyl-4-deuteriobenzene
• CAS No.: 72302-30-8
• Molecular Formula: C₁₀H₁₄
• Molecular Weight: 135.213
• Mol file: 72302-30-8.mol

Synonyms:1-butyl-4-deuteriobenzene

Chemical Property of 1-butyl-4-deuteriobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-butyl-4-deuteriobenzene

There total 7 articles about 1-butyl-4-deuteriobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

4-butyliodobenzene (20651-67-6) → 1-butyl-4-deuteriobenzene (72302-30-8)

Guidance literature:

With copper(I) trifluoromethanesulfonate bis(trimethylacetonitrile) complex; water-d2; silver fluoride; In N,N-dimethyl-formamide; at 140 ℃; for 22h; Inert atmosphere;

DOI:10.1021/ja304410x

Reference yield: 76.0%

4-butylphenylboronic acid (145240-28-4) → 1-butyl-4-deuteriobenzene (72302-30-8)

Guidance literature:

With water-d2; sodium hydroxide; In di-isopropyl ether; acetonitrile; at 25 ℃; for 24h; Inert atmosphere; UV-irradiation; Green chemistry;

DOI:10.1039/d0gc01649g

Reference yield: 74.0%

4-n-butyl-1-trimethylsilylbenzene (81631-74-5) → 1-butyl-4-deuteriobenzene (72302-30-8)

Guidance literature:

With supercritical D₂O; at 390 ℃; for 0.5h; under 202516 Torr;

DOI:10.1021/ja034227g

upstream raw materials:

4-n-butyl-1-trimethylsilylbenzene

1.4-dibromobenzene

1-bromo-4-(trimethylsilyl)benzene

4-butyliodobenzene