Technology Process of C62H44N2O12S2
There total 5 articles about C62H44N2O12S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / aq. NaOH, tri-n-butylbenzylammonium chloride / CH2Cl2 / 1.5 h
2: 90 percent / Et2NH / CHCl3 / 48 h
3: K2CO3 / acetone / 24 h / Heating
With
sodium hydroxide; benzyltri(n-butyl)ammonium chloride; potassium carbonate; diethylamine;
In
dichloromethane; chloroform; acetone;
DOI:10.1021/ja00184a044
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 47 percent / NBS / CCl4 / 21 h / Heating; Irradiation
2: 70 percent / aq. NaOH, tri-n-butylbenzylammonium chloride / CH2Cl2 / 1.5 h
3: 90 percent / Et2NH / CHCl3 / 48 h
4: K2CO3 / acetone / 24 h / Heating
With
sodium hydroxide; N-Bromosuccinimide; benzyltri(n-butyl)ammonium chloride; potassium carbonate; diethylamine;
In
tetrachloromethane; dichloromethane; chloroform; acetone;
DOI:10.1021/ja00184a044
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / aq. NaOH, tri-n-butylbenzylammonium chloride / CH2Cl2 / 1.5 h
2: 90 percent / Et2NH / CHCl3 / 48 h
3: K2CO3 / acetone / 24 h / Heating
With
sodium hydroxide; benzyltri(n-butyl)ammonium chloride; potassium carbonate; diethylamine;
In
dichloromethane; chloroform; acetone;
DOI:10.1021/ja00184a044