N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt

Base Information

Chemical Name:N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt
CAS No.:122410-35-9
Molecular Formula:C₂₆H₂₆NO₅*Na
Molecular Weight:455.486
Hs Code.:

Synonyms:N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt

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Chemical Property of N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt

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Technology Process of N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt

There total 5 articles about N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 37491-68-2
3,4-dihydroxybenzylamine

: 105226-92-4
(S,S)-2,4-dibenzylglutaric anhydride

: 122410-35-9
N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt

Guidance literature:: With pyridine; sodium hydroxide; 1) CH₂Cl₂, r. t., 16 h;
DOI:10.1021/jm00132a005

Reference yield:

: 105129-13-3
threo-2,4-dibenzylglutaric acid

: 122410-35-9
N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt

Guidance literature:: Multi-step reaction with 5 steps

1: acetyl chloride / toluene / 2 h

2: 15percent Et₃N / toluene / 0.25 h / 50 °C

3: H₂O / dioxane / Heating

4: 98 percent / Ac₂O / toluene / 2 h

5: 84 percent / 1) pyridine, 2) 1 N NaOH / 1) CH₂Cl₂, r. t., 16 h

With pyridine; sodium hydroxide; water; acetic anhydride; triethylamine; acetyl chloride; In 1,4-dioxane; toluene;
DOI:10.1021/jm00132a005

Reference yield:

: 105129-11-1
cis-2,4-dibenzylglutaric anhydride

: 122410-35-9
N-<(S,S)-2,4-dibenzyl-4-carboxybutyryl>-3,4-dihydroxybenzylamine sodium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 15percent Et₃N / toluene / 0.25 h / 50 °C

2: H₂O / dioxane / Heating

3: 98 percent / Ac₂O / toluene / 2 h

4: 84 percent / 1) pyridine, 2) 1 N NaOH / 1) CH₂Cl₂, r. t., 16 h

With pyridine; sodium hydroxide; water; acetic anhydride; triethylamine; In 1,4-dioxane; toluene;
DOI:10.1021/jm00132a005