N,N-dibenzyl-4-bromobenzenesulfonamide

Base Information

Chemical Name:N,N-dibenzyl-4-bromobenzenesulfonamide
CAS No.:5265-55-4
Molecular Formula:C20H18BrNO2S
Molecular Weight:416.3314
Hs Code.:
DSSTox Substance ID:DTXSID60362419
Wikidata:Q82145479
Mol file:5265-55-4.mol

Synonyms:N,N-dibenzyl-4-bromobenzenesulfonamide;Oprea1_177488;Oprea1_422723;DTXSID60362419;STK325784;AKOS000383632;AB00027027-01;Z45508889

Suppliers and Price of N,N-dibenzyl-4-bromobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of N,N-dibenzyl-4-bromobenzenesulfonamide

Chemical Property:

Vapor Pressure:6.39E-12mmHg at 25°C
Boiling Point:544.6°C at 760 mmHg
Flash Point:283.2°C
Density:1.423g/cm³
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:415.02416
Heavy Atom Count:25
Complexity:464

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CN(CC2=CC=CC=C2)S(=O)(=O)C3=CC=C(C=C3)Br

Technology Process of N,N-dibenzyl-4-bromobenzenesulfonamide

There total 13 articles about N,N-dibenzyl-4-bromobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 102562-17-4
2',3'-di-O-acetyl-2,6,8-tris<(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

: 21082-30-4,5265-55-4
9-β-(D-ribofuranosyl)-1H-purine-2,6,8(3H,7H,9H)-trione

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; at 100 ℃; for 1.5h;
DOI:10.1002/hlca.19870700126

Reference yield: 70.0%

: 3868-37-9
8-benzyloxy-xanthosine

: 21082-30-4,5265-55-4
9-β-(D-ribofuranosyl)-1H-purine-2,6,8(3H,7H,9H)-trione

Guidance literature:: With palladium on carbon; hydrogen;
DOI:10.1016/j.tetlet.2010.11.123

Reference yield:

: 118-00-3
G

: 21082-30-4,5265-55-4
9-β-(D-ribofuranosyl)-1H-purine-2,6,8(3H,7H,9H)-trione

Guidance literature:: Multi-step reaction with 8 steps

1: 1.)bromination reagent

2: 84 percent / PPh₃, EtOOC-N=N-COOEt

3: 93 percent / nitrosus acid / acetone; H₂O / 10 °C

4: 90 percent / Ag⁽¹⁺⁾

5: 92 percent / NaOOCCH₃ / acetic acid / Heating

6: 88 percent / Ag⁽¹⁺⁾

7: DBU / pyridine

8: NH₃

With bromination reagent; ammonia; sodium acetate; cis-nitrous acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; diethylazodicarboxylate; silver (I) ion; In pyridine; water; acetic acid; acetone;
DOI:10.1016/S0040-4039(00)98224-8