dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate

Base Information

Chemical Name:dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate
CAS No.:1242096-25-8
Molecular Formula:C₂₁H₃₀O₇
Molecular Weight:394.465
Hs Code.:

Synonyms:dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate

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Chemical Property of dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate

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Technology Process of dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate

There total 2 articles about dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 31469-15-5
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

: 1242096-12-3
dimethyl 3-(3,4-dimethoxyphenyl)-2,2-dimethylpentane-1,5-dioate

: 1242096-25-8
dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 20 - 25 ℃; Inert atmosphere;
DOI:10.1039/c0cc01110j

Reference yield: 48.0%

: 31469-15-5
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

: 2316-26-9
3,4-dimethoxycinnamic acid

: 1242096-25-8
dimethyl 2,2,6,6-tetramethyl-3-oxo-5-(3,4-dimethoxyphenyl)-1,7-heptanedioate

Guidance literature:: 1-methoxy-2-methyl-1-trimethylsiloxy-1-propene; 3,4-dimethoxycinnamic acid; With sodium hydroxide; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 3h; Inert atmosphere;

With hydrogenchloride; methanol; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 0.5h;
DOI:10.1039/c0cc01110j