allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate

Base Information

Chemical Name:allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate
CAS No.:162795-40-6
Molecular Formula:C₂₆H₃₅NO₆S₂Si
Molecular Weight:549.785
Hs Code.:

Synonyms:allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate

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Chemical Property of allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate

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Technology Process of allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate

There total 1 articles about allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 88585-78-8
<4S,5R,6S(R)>-3-(hydroxymethyl)-6-<1-<(tert-butyldimethylsilyl)oxy>ethyl>-7-oxo-4-thia-1-azabicyclo<3.2.0>hept-2-enecarboxylic acid 2-allyl ester

: 62167-01-5
phenoxythiolacetic acid

: 162795-40-6
allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;
DOI:10.1080/00397919508011770

Reference yield:

: 162795-40-6
allyl (5R,6S)-2-(phenoxyacetylthiomethyl)-6-<(1R)-1-tert-butyldimethylsssilyloxyethyl>-penem-3-carboxylate

: 2065-23-8
methyl 2-phenoxyacetate

: (5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-mercaptomethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid allyl ester

: (5R,6S)-6-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-3-[1-mercapto-meth-(Z)-ylidene]-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid allyl ester

Guidance literature:: With sodium methylate; In methanol; at -25 ℃; for 0.5h; Title compound not separated from byproducts;
DOI:10.1080/00397919508011770