tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate

Base Information

Chemical Name:tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate
CAS No.:1187224-05-0
Molecular Formula:C₂₄H₃₄N₂O₅
Molecular Weight:430.544
Hs Code.:

Synonyms:tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate

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Chemical Property of tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate

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Technology Process of tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate

There total 5 articles about tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1187224-04-9
(S)-3 ((S)-2-azido-2-((1r,4S)-4-methylcyclohexyl)acetyl)-4-benzyloxazolidin-2-one

: 1187224-05-0
tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In N,N-dimethyl-formamide; for 4h;

Reference yield:

: 1187224-03-8
(S)-4-benzyl-3-(2-((1r,4S)-4-methylcyclohexyl)acetyl)oxazolidin-2-one

: 1187224-05-0
tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -70 °C / Inert atmosphere

1.2: 1.13 h / -70 °C / Inert atmosphere

1.3: -70 - 30 °C

2.1: hydrogen / palladium 10% on activated carbon / N,N-dimethyl-formamide / 4 h

With hydrogen; potassium hexamethylsilazane; palladium 10% on activated carbon; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: trans-(4-methylcyclohexyl)acetic acid

: 1187224-05-0
tert-butyl (S)-2-((S)-4-benzyl-2-oxooxazolidin-3-yl)-1-((1r,4S)-4-methylcyclohexyl)-2-ooxoethylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran / -78 - 0 °C

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: 5.08 h / -78 - 20 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -70 °C / Inert atmosphere

3.2: 1.13 h / -70 °C / Inert atmosphere

3.3: -70 - 30 °C

4.1: hydrogen / palladium 10% on activated carbon / N,N-dimethyl-formamide / 4 h

With n-butyllithium; hydrogen; potassium hexamethylsilazane; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;