5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten

Base Information

• Chemical Name: 5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten
• CAS No.: 102451-64-9
• Molecular Formula: C₂₂H₁₇BrO₃S
• Molecular Weight: 441.345

Synonyms:5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten

Chemical Property of 5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten

Chemical Property:

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Technology Process of 5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten

There total 3 articles about 5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5H-dibenzocycloheptene-5-carboxaldehyde (1605-13-6) → 5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten (102451-64-9)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

2: Py

With pyridine; lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/ja01508a046

Reference yield:

C16H12O → 5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten (102451-64-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂O / 140 °C

2: LiAlH₄ / diethyl ether

3: Py

With pyridine; lithium aluminium tetrahydride; water; In diethyl ether;

DOI:10.1021/ja01508a046

Reference yield:

(5H-dibenzo[a,d]cyclohepten-5-yl)-methanol (2975-62-4) + 4-bromobenzenesulfonyl chloride (98-58-8) → 5-<4-Brom-benzolsulfonyloxymethyl>-5H-dibenzocyclohepten (102451-64-9)

Guidance literature:

With pyridine;

DOI:10.1021/ja01508a046

upstream raw materials:

(5H-dibenzo[a,d]cyclohepten-5-yl)-methanol

4-bromobenzenesulfonyl chloride

5H-dibenzocycloheptene-5-carboxaldehyde

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