1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene

Base Information

Chemical Name:1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene
CAS No.:404875-14-5
Molecular Formula:C₂₀H₄₂Cl₄Si₄Sn₂
Molecular Weight:774.127
Hs Code.:

Synonyms:1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene

Chemical Property:

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Technology Process of 1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene

There total 3 articles about 1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 404875-13-4
1,4-bis(((trimethylsilylmethyl)diphenylstannylmethyl)dimethylsilyl)benzene

: mercury dichloride

: 404875-14-5
1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene

Guidance literature:: In acetone; byproducts: C6H5HgCl; to a stirred soln. (0°C) of complex in acetone was added dropwisea soln. of HgCl2 in acetone over 30 min, the mixt. was stirred overnigh t; C6H5HgCl was filtered off, acetone was removed in vac., diethyl ether was added, the suspn. was stirred for 10 min, C6H5HgCl was filtered, evapd., recrystd. from diethyl ether-hexane; elem. anal.;
DOI:10.1021/om0105627

Reference yield:

: 503815-75-6
1,4-bis((iododimethylstannylmethyl)dimethylsilyl)benzene

: 404875-14-5
1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: acetone

In tetrahydrofuran; acetone;
DOI:10.1021/om0105627

Reference yield:

: 404875-11-2
1,4-bis((triphenylstannylmethyl)dimethylsilyl)benzene

: 404875-14-5
1,4-bis(((trimethylsilylmethyl)dichlorostannylmethyl)dimethylsilyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran

2: tetrahydrofuran

3: acetone

In tetrahydrofuran; acetone;
DOI:10.1021/om0105627