Technology Process of C17H13NS2
There total 3 articles about C17H13NS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H17NS2;
With
sodium tert-butyl thiolate;
In
N,N-dimethyl-formamide;
at 160 ℃;
for 4h;
Inert atmosphere;
With
hydrogenchloride;
In
N,N-dimethyl-formamide;
at 0 ℃;
Inert atmosphere;
DOI:10.1021/om300789h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate / 1,2-dimethoxyethane; water / 12 h / 85 °C / Schlenk technique; Sealed tube
2.1: sodium tert-butyl thiolate / N,N-dimethyl-formamide / 4 h / 160 °C / Inert atmosphere
2.2: 0 °C / Inert atmosphere
With
trans-bis(triphenylphosphine)palladium dichloride; sodium tert-butyl thiolate; potassium carbonate;
In
1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
1.1: |Suzuki Coupling;
DOI:10.1021/om300789h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate / 1,2-dimethoxyethane; water / 12 h / 85 °C / Schlenk technique; Sealed tube
2.1: sodium tert-butyl thiolate / N,N-dimethyl-formamide / 4 h / 160 °C / Inert atmosphere
2.2: 0 °C / Inert atmosphere
With
trans-bis(triphenylphosphine)palladium dichloride; sodium tert-butyl thiolate; potassium carbonate;
In
1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
1.1: |Suzuki Coupling;
DOI:10.1021/om300789h
