N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

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Chemical Name:N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside
CAS No.:1429920-37-5
Molecular Formula:C₁₀₂H₁₀₇Cl₃N₂O₁₉
Molecular Weight:1771.33
Hs Code.:

N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

Synonyms:N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

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Chemical Property of N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

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Technology Process of N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

There total 1 articles about N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1429920-36-4
ethyl 6-O-acetyl-2,4-di-O-benzyl-3-O-(2-naphthylmethyl)-1-thio-β-D-glucopyranoside

: N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-2,3,6-tri-O-benzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

: 1429920-37-5
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: ethyl 6-O-acetyl-2,4-di-O-benzyl-3-O-(2-naphthylmethyl)-1-thio-β-D-glucopyranoside; N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-2,3,6-tri-O-benzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside; With N-iodo-succinimide; In diethyl ether; dichloromethane; at -50 ℃; for 0.25h; Inert atmosphere; Molecular sieve;

With trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at -50 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.201204394

Reference yield:

: 1429920-37-5
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside

: C₁₀₀H₁₀₅Cl₃N₂O₁₈

Guidance literature:: N-(benzyl)benzyloxycarbonyl-5-aminopentanyl-6-O-acetyl-2,4-di-Obenzyl-3-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1→4)-2,3,6-tri-Obenzyl-α-D-galactopyranosyl-(1→3)-4,6-di-O-benzyl-2-trichloroacetamido-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃; for 3h; Inert atmosphere;

In methanol; pH=6; Inert atmosphere;
DOI:10.1002/chem.201204394