C₄₄H₇₃Si₃O₅N₃

Base Information

Chemical Name:C₄₄H₇₃Si₃O₅N₃
CAS No.:930807-80-0
Molecular Formula:C₄₄H₇₃N₃O₅Si₃
Molecular Weight:808.337
Hs Code.:

C<sub>44</sub>H<sub>73</sub>Si<sub>3</sub>O<sub>5</sub>N<sub>3</sub>

Synonyms:C₄₄H₇₃Si₃O₅N₃

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Chemical Property of C₄₄H₇₃Si₃O₅N₃

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Technology Process of C₄₄H₇₃Si₃O₅N₃

There total 7 articles about C₄₄H₇₃Si₃O₅N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 930807-79-7
C₄₄H₇₄Si₃O₆

: 930807-80-0
C₄₄H₇₃Si₃O₅N₃

Guidance literature:: With diphenylphosphoranyl azide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃; for 2h;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-76-4
C₄₀H₆₂Si₂O₇

: 930807-80-0
C₄₄H₇₃Si₃O₅N₃

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / ethyl pivalate / tetrahydrofuran; toluene / 15 h / 80 °C

2: 93 percent / p-toluenesulfonic acid / methanol / 1.5 h / 40 °C

3: 76 percent / imidazole / CH₂Cl₂ / 0.5 h / -78 °C

4: 88 percent / triphenylphosphine; diphenylphosphorylazide; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 20 °C

With 1H-imidazole; 2,2-dimethyl-propanoic acid ethyl ester; diphenylphosphoranyl azide; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 4: Mitsunobu reaction;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-74-2
C₃₄H₅₀O₇Si

: 930807-80-0
C₄₄H₇₃Si₃O₅N₃

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 1.25 h / -78 °C

2: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 2 h / 20 °C

3: 77 percent / ethyl pivalate / tetrahydrofuran; toluene / 15 h / 80 °C

4: 93 percent / p-toluenesulfonic acid / methanol / 1.5 h / 40 °C

5: 76 percent / imidazole / CH₂Cl₂ / 0.5 h / -78 °C

6: 88 percent / triphenylphosphine; diphenylphosphorylazide; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; 2,2-dimethyl-propanoic acid ethyl ester; diphenylphosphoranyl azide; Dess-Martin periodane; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 2: Dess-Martin oxidation / 6: Mitsunobu reaction;
DOI:10.1002/anie.200603656