Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester

Base Information

Chemical Name:Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester
CAS No.:125237-60-7
Molecular Formula:C₂₄H₃₇NO₄S
Molecular Weight:435.628
Hs Code.:

Synonyms:Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester

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Technology Process of Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester

There total 1 articles about Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 455-16-3
p-toluenesulfonyl fluoride

: 125237-55-0
(E)-3,7-dimethylocta-2,6-dienyl N,N-diisopropylcarbamate

: 125237-60-7
Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at -70 ℃; for 2h;
DOI:10.1016/S0040-4039(00)99157-3

Reference yield:

: 81445-44-5
(S)-2-(benzyloxy)propanal

: 125237-60-7
Diisopropyl-carbamic acid (E)-3,7-dimethyl-1-(toluene-4-sulfonyl)-octa-2,6-dienyl ester

: 125285-09-8
Diisopropyl-carbamic acid (E)-(R)-1-((S)-1-benzyloxy-ethyl)-4,8-dimethyl-2-oxo-nona-3,7-dienyl ester

Guidance literature:: With titanium(IV) isopropylate; n-butyllithium; hexane; Yield given. Multistep reaction; 1.) THF, -78 deg C, 5.5 h;
DOI:10.1016/S0040-4039(00)99158-5