(S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate

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Chemical Name:(S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate
CAS No.:1390672-76-0
Molecular Formula:C₃₂H₃₈N₄O₃S
Molecular Weight:558.745
Hs Code.:

Synonyms:(S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate

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Chemical Property of (S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate

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Technology Process of (S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate

There total 5 articles about (S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1390672-74-8
(S)-(9H-fluoren-9-yl)methyl 2-[(1S,2S)-2-{3-[(S)-2-tert-butoxy-2-oxo-1-phenylethyl]thioureido}-1,2-diphenylethylcarbamoyl]pyrrolidine-1-carboxylate

: 1390672-76-0
(S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1039/c2ob25693b

Reference yield:

: 1390672-72-6
C₁₃H₁₅NO₂S

: 1390672-76-0
(S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 18 h / 20 °C

2: piperidine / N,N-dimethyl-formamide / 1 h / 20 °C

With piperidine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25693b

Reference yield:

: 1390672-71-5
(S)-(9H-fluoren-9-yl)methyl 2-[(1S,2S)-2-amino-1,2-diphenylethylcarbamoyl]pyrrolidine-1-carboxylate

: 1390672-76-0
(S)-tert-butyl 2-{3-[(1S,2S)-1,2-diphenyl-2-[(S)-pyrrolidine-2-carboxamido]ethyl]thioureido}-2-phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 18 h / 20 °C

2: piperidine / N,N-dimethyl-formamide / 1 h / 20 °C

With piperidine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25693b