1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

Base Information

Chemical Name:1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane
CAS No.:70057-34-0
Molecular Formula:C₄₀H₅₆Si₆
Molecular Weight:705.398
Hs Code.:

1,1,2,2-tetraphenyl-3-<bis(trimethylsilyl)ethenylidene>-4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

Synonyms:1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

Chemical Property:

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Technology Process of 1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

There total 4 articles about 1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 70057-33-9
1,1,2,2-tetraphenyl-3,4-bis-1,2-disilacyclobutane

: 70057-34-0
1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

Guidance literature:: at 200 ℃; for 3h; sealed tube;
DOI:10.1021/ja00399a031

Reference yield:

: 61211-96-9
1-chloro-1,1-diphenyl-2,2,2-trimethyldisilane

: 70057-34-0
1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) magnesium, ethyl bromide / 1.) THF, room temperature, 1 h, 2.) reflux, 4 h

2: 29 percent / 5 h / Irradiation

3: 99 percent / 3 h / 200 °C / sealed tube

With ethyl bromide; magnesium;
DOI:10.1021/ja00399a031

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 70057-34-0
1,1,2,2-tetraphenyl-3--4,4-bis(trimethylsilyl)-1,2-disilacyclobutane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) magnesium, ethyl bromide / 1.) THF, room temperature, 1 h, 2.) reflux, 4 h

2: 29 percent / 5 h / Irradiation

3: 99 percent / 3 h / 200 °C / sealed tube

With ethyl bromide; magnesium;
DOI:10.1021/ja00399a031