N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide

Base Information

Chemical Name:N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide
CAS No.:93887-24-2
Molecular Formula:C₂₈H₃₄N₆O₅S*HI
Molecular Weight:694.594
Hs Code.:

Synonyms:N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide

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Chemical Property of N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide

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Technology Process of N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide

There total 9 articles about N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 93887-12-8
4-(2-Butylcarbamoyl-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-ethyl)-thiobenzimidic acid methyl ester; hydriodide

: 93887-24-2
N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide

Guidance literature:: With ammonium acetate; In methanol; at 60 ℃; for 3h;

Reference yield:

: 92740-47-1
α-naphthylenesulfonylglycine

: 93887-24-2
N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide

Guidance literature:: Multi-step reaction with 9 steps

1: SOCl₂ / 1 h / Heating

2: 2 M NaOH / CHCl₃; ethyl acetate / 10 h

3: 70 percent / DCC / pyridine; ethyl acetate / 1.) 2 h, 2.) 10 h, room temperature

4: 75 percent / Et₃N / pyridine; ethyl acetate / 2 h

5: DCC / pyridine; ethyl acetate / 1.) 2 h, 2.) 10 h, room temperature

6: CHCl₃ / 2 h

7: 60 percent / H₂S, TEA / pyridine / Ambient temperature

8: 55 percent / acetone / 0.17 h / Heating

9: 60 percent / CH₃COONH₄ / methanol / 3 h / 60 °C

With sodium hydroxide; thionyl chloride; TEA; hydrogen sulfide; ammonium acetate; triethylamine; dicyclohexyl-carbodiimide; In pyridine; methanol; chloroform; ethyl acetate; acetone;

Reference yield:

: 93886-71-6
1-Naphthylsulfonylglycylglycin

: 93887-24-2
N-Butyl-3-(4-carbamimidoyl-phenyl)-2-{2-[2-(naphthalene-1-sulfonylamino)-acetylamino]-acetylamino}-propionamide; hydriodide

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / DCC / pyridine; ethyl acetate / 1.) 2 h, 2.) 10 h, room temperature

2: 75 percent / Et₃N / pyridine; ethyl acetate / 2 h

3: DCC / pyridine; ethyl acetate / 1.) 2 h, 2.) 10 h, room temperature

4: CHCl₃ / 2 h

5: 60 percent / H₂S, TEA / pyridine / Ambient temperature

6: 55 percent / acetone / 0.17 h / Heating

7: 60 percent / CH₃COONH₄ / methanol / 3 h / 60 °C

With TEA; hydrogen sulfide; ammonium acetate; triethylamine; dicyclohexyl-carbodiimide; In pyridine; methanol; chloroform; ethyl acetate; acetone;