1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol

Base Information

Chemical Name:1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol
CAS No.:613234-38-1
Molecular Formula:C₆₀H₅₄N₂O₅
Molecular Weight:883.099
Hs Code.:

Synonyms:1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol

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Chemical Property of 1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol

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Technology Process of 1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol

There total 7 articles about 1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 76-83-5
trityl chloride

: 426824-63-7
1,3-di-O-benzyl-1-[1H-imidazol-4⁽⁵⁾-yl]-L-gulo-pentitol

: 613234-38-1
1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol

Guidance literature:: With pyridine; dmap; at 80 ℃;
DOI:10.1016/S0040-4039(01)02320-6

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 613234-38-1
1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.25 h / -70 °C

1.2: 47 percent / hexane; tetrahydrofuran / 2.75 h / -70 - 20 °C

2.1: NaH / dimethylformamide; various solvent(s) / 0 - 20 °C

3.1: 1.06 g / hydrochloric acid / H₂O; tetrahydrofuran / 1.5 h / Heating

4.1: 87 percent / NaBH₄ / methanol / 0 - 20 °C

5.1: 48 percent / 4-(dimethylamino)pyridine; pyridine / 48 h / 80 - 90 °C

With pyridine; hydrogenchloride; dmap; sodium tetrahydroborate; n-butyllithium; sodium hydride; In tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)01055-X

Reference yield:

: (5R)-3,5-di-O-benzyl-5-[1H-imidazol-4⁽⁵⁾-yl]-D-xylofuranose

: 613234-38-1
1,3-di-O-benzyl-1-(1-triphenylmethyl-1H-imidazol-4-yl)-5-O-triphenylmethyl-L-gulo-pentitol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaBH₄ / methanol / 0 - 20 °C

2: 48 percent / 4-(dimethylamino)pyridine; pyridine / 48 h / 80 - 90 °C

With pyridine; dmap; sodium tetrahydroborate; In methanol;
DOI:10.1016/S0040-4020(03)01055-X