Technology Process of diethyl 3,3-bis(benzylthio)glutarate
There total 1 articles about diethyl 3,3-bis(benzylthio)glutarate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
titanium tetrachloride;
In
dichloromethane;
for 36h;
Ambient temperature;
DOI:10.1021/ja00104a004
- Guidance literature:
-
With
sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran; toluene;
at 0 ℃;
for 1h;
DOI:10.1021/ja00104a004
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / sodium bis(2-methoxyethoxy)aluminum hydride / toluene; tetrahydrofuran / 1 h / 0 °C
2: N,N-diisopropylethylamine / CH2Cl2 / 2 h / Ambient temperature
3: N,N-diisopropylethylamine / acetone / 8 h / Heating
4: NH3 (g) / ethanol / 1 h / Ambient temperature
With
ammonia; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran; ethanol; dichloromethane; acetone; toluene;
DOI:10.1021/ja00104a004
