((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

Base Information

• Chemical Name: ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene
• CAS No.: 1204221-12-4
• Molecular Formula: C₅₀H₄₉ClO₄
• Molecular Weight: 750.382

Synonyms:((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

Chemical Property of ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

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Technology Process of ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

There total 1 articles about ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

(1R,4R,5S,6R)-4,5,6-tris(benzyloxy)-3-(benzyloxymethyl)-1-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-2-enol (1161430-09-6) → ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene (1204221-12-4)

Guidance literature:

With Et₃SiD; boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃;

Reference yield: 46.7%

((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene (1204221-12-4) → (1R,2R,3S,4S,6R)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)-6-(hydroxymethyl)cyclohexane-6-d-1,2,3-triol

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; for 3h;

Reference yield: 22.9%

((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-4-ene-6-d-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene (1204221-12-4) → (1R,2R,3S,4R,5R,6S)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)-6-(hydroxymethyl)cyclohexane-6-d-1,2,3,5-tetraol (1204221-30-6)

Guidance literature:

With hydrogen; 1,2-dichloro-benzene; palladium 10% on activated carbon; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

upstream raw materials:

(1R,4R,5S,6R)-4,5,6-tris(benzyloxy)-3-(benzyloxymethyl)-1-(4-chloro-3-(4-ethylbenzyl)phenyl)cyclohex-2-enol

Downstream raw materials:

(1R,2R,3S,4R,5R,6S)-4-(4-chloro-3-(4-ethylbenzyl)phenyl)-6-(hydroxymethyl)cyclohexane-6-d-1,2,3,5-tetraol

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