(4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole

Base Information

Chemical Name:(4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole
CAS No.:1100555-10-9
Molecular Formula:C₁₇H₂₀N₂O₅
Molecular Weight:332.356
Hs Code.:

Synonyms:(4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole

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Chemical Property of (4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole

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Technology Process of (4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole

There total 2 articles about (4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3-crotonoyl-5,5-dimethyl-2-oxazolidinone

: 38435-51-7
N-hydroxy-4-methoxy-benzenecarboximidoyl chloride

: 1100555-10-9
(4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole

Guidance literature:: With nickel(II) perchlorate hexahydrate; (R)-N,N'-bis(4-phenyl-2-quinolylmethylene)-1,1'-binaphthyl-2,2'-diamine; In dichloromethane; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo802392c

Reference yield:

: 3-crotonoyl-5,5-dimethyl-2-oxazolidinone

: 38435-51-7
N-hydroxy-4-methoxy-benzenecarboximidoyl chloride

: (4R,5R)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole

: 1100555-10-9
(4S,5S)-5-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-4-methyl-4,5-dihydroisoxazole

: 4-[(5,5-dimethyl-2-oxo-3-oxazolidinyl)carbonyl]-3-(p-methoxyphenyl)-5-methyl-4,5-dihydroisoxazole

Guidance literature:: With nickel(II) perchlorate hexahydrate; (R)-N,N'-bis(4-phenyl-2-quinolylmethylene)-1,1'-binaphthyl-2,2'-diamine; In dichloromethane; at 20 ℃; for 43h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo802392c