ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate

Base Information

Chemical Name:ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate
CAS No.:1428765-51-8
Molecular Formula:C₁₇H₂₆N₂O₆S
Molecular Weight:386.469
Hs Code.:

Synonyms:ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate

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Chemical Property of ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate

Chemical Property:

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Technology Process of ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate

There total 6 articles about ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1119363-04-0
N-(1-(N-(tert-butoxycarbonyl)sulfamoyl)pyridin-4(1H)-ylidene)-N-methylmethanaminium

: 1428765-50-7
ethyl 2-(4-(aminomethyl)phenyl)propanoate

: 1428765-51-8
ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1878-68-8
2-(4-bromophenyl)-acetic acid

: 1428765-51-8
ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / Reflux

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 4 h / 0 - 20 °C

4.1: palladium on carbon; hydrogen / ethanol / 18 h / 20 °C / 3102.97 Torr

5.1: trifluoroacetic acid / dichloromethane / 4 h / 0 - 20 °C

6.1: dichloromethane / 16 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; palladium on carbon; hydrogen; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 118618-32-9
ethyl 2-(p-cyano-phenyl)-propionate

: 1428765-51-8
ethyl 2-(4-((N-(tert-butoxycarbonyl)sulfamoylamino)methyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on carbon; hydrogen / ethanol / 18 h / 20 °C / 3102.97 Torr

2: trifluoroacetic acid / dichloromethane / 4 h / 0 - 20 °C

3: dichloromethane / 16 h / 20 °C

With palladium on carbon; hydrogen; trifluoroacetic acid; In ethanol; dichloromethane;