N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

Base Information

Chemical Name:N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline
CAS No.:80957-34-2
Molecular Formula:C₂₆H₃₈N₄O₈S
Molecular Weight:566.676
Hs Code.:

N-(t-butoxycarbonyl)glycyl-<S-(p-methoxybenzyl)-L-cysteinyl>sarcosyl-L-proline

Synonyms:N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

Suppliers and Price of N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

There total 5 articles about N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 80957-33-1
Boc-Gly-L-Cys(Bzl(OMe))-Sar-L-Pro-OMe

: 80957-34-2
N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

Guidance literature:: With sodium hydroxide; In methanol; for 1.5h;
DOI:10.1246/bcsj.55.3808

Reference yield:

: 80957-29-5
N-(t-butoxycarbonyl)sarcosyl-L-proline methyl ester

: 80957-34-2
N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / HCl / ethyl acetate / 1 h / Ambient temperature

2: 84 percent / DCC / CHCl₃ / a) -5 deg C, 5 h, b) RT, overnight

3: 100 percent / HCl / ethyl acetate / 1 h / Ambient temperature

4: 73 percent / DCC / CHCl₃ / a) -5 deg C, 5 h, b) RT, overnight

5: 89 percent / NaOH / methanol / 1.5 h

With hydrogenchloride; sodium hydroxide; dicyclohexyl-carbodiimide; In methanol; chloroform; ethyl acetate;
DOI:10.1246/bcsj.55.3808

Reference yield:

: sarcosyl-L-proline methyl ester hydrochloride

: 80957-34-2
N-(t-butoxycarbonyl)glycyl-sarcosyl-L-proline

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / DCC / CHCl₃ / a) -5 deg C, 5 h, b) RT, overnight

2: 100 percent / HCl / ethyl acetate / 1 h / Ambient temperature

3: 73 percent / DCC / CHCl₃ / a) -5 deg C, 5 h, b) RT, overnight

4: 89 percent / NaOH / methanol / 1.5 h

With hydrogenchloride; sodium hydroxide; dicyclohexyl-carbodiimide; In methanol; chloroform; ethyl acetate;
DOI:10.1246/bcsj.55.3808