(2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate

Base Information

Chemical Name:(2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate
CAS No.:1258539-82-0
Molecular Formula:C₄₆H₄₉NO₈
Molecular Weight:743.897
Hs Code.:

Synonyms:(2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate

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Chemical Property of (2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate

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Technology Process of (2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate

There total 1 articles about (2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1258539-81-9
benzyl (2R,3S,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-(3-methoxy-3-oxoprop-1-en-1-yl)piperidine-1-carboxylate

: 1258539-82-0
(2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate

Guidance literature:: With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; dichloromethane; at 0 - 20 ℃; for 5h;
DOI:10.1039/c0ob00042f

Reference yield:

: 1258539-82-0
(2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate

: C₄₅H₄₇NO₈

Guidance literature:: (2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)methyl propionate; With sodium hydroxide; In methanol; water; at 60 ℃; for 5h;

In methanol; water; pH=5 - 6;
DOI:10.1039/c0ob00042f