C₃₃H₂₅ClO₂

Base Information

Chemical Name:C₃₃H₂₅ClO₂
CAS No.:246227-81-6
Molecular Formula:C₃₃H₂₅ClO₂
Molecular Weight:489.013
Hs Code.:

C<sub>33</sub>H<sub>25</sub>ClO<sub>2</sub>

Synonyms:C₃₃H₂₅ClO₂

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Chemical Property of C₃₃H₂₅ClO₂

Chemical Property:

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Technology Process of C₃₃H₂₅ClO₂

There total 1 articles about C₃₃H₂₅ClO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 246227-80-5
C₃₃H₂₆O₃

: 246227-81-6
C₃₃H₂₅ClO₂

Guidance literature:: With pyridine; thionyl chloride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jo9911903

Reference yield:

: 246227-81-6
C₃₃H₂₅ClO₂

: 246227-83-8
C₃₃H₂₆O₂

Guidance literature:: With sodium tetrahydroborate; In sulfolane; at 100 ℃; for 1h;
DOI:10.1021/jo9911903

Reference yield:

: 246227-81-6
C₃₃H₂₅ClO₂

: 246227-85-0
C₂₈H₁₆O

Guidance literature:: Multi-step reaction with 2 steps

1: 1.144 g / sodium borohydride / tetrahydrothiophene 1,1-dioxide / 1 h / 100 °C

2: 93 percent / p-toluenesulfonic acid monohydrate / acetone; tetrahydrofuran; H₂O / 23 h / 56 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; In tetrahydrofuran; sulfolane; water; acetone; 1: Reduction / 2: Hydrolysis;
DOI:10.1021/jo9911903