6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester

Base Information

• Chemical Name: 6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester
• CAS No.: 1235975-83-3
• Molecular Formula: C₁₅H₁₈ClN₃O₆
• Molecular Weight: 371.777

Synonyms:6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester

Chemical Property of 6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester

Chemical Property:

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Technology Process of 6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester

There total 1 articles about 6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-3-nitro-benzoyl isocyanate + methyl 6-aminocaproate hydrochloride (1926-80-3) → 6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester (1235975-83-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;

DOI:10.1016/j.bmcl.2010.04.041

Reference yield: 73.0%

1-(2-aminoethyl)pyrrolidine (7154-73-6) + 6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester (1235975-83-3) → C21H31N5O6 (1235976-13-2)

Guidance literature:

With triethylamine; In 1,4-dioxane; at 80 ℃; for 8.5h;

DOI:10.1016/j.bmcl.2010.04.041

Reference yield:

6-[3-(4-chloro-3-nitro-benzoyl)-ureido]-hexanoic acid methyl ester (1235975-83-3) → C15H20ClN3O4 (1235976-06-3)

Guidance literature:

With tin(II) chloride dihdyrate; In methanol; dichloromethane; at 20 ℃;

DOI:10.1016/j.bmcl.2010.04.041

upstream raw materials:

methyl 6-aminocaproate hydrochloride

Downstream raw materials:

C₁₉H₂₆N₄O₆

C₂₀H₂₈N₄O₆

C₁₉H₂₆N₄O₇

C₂₀H₂₉N₅O₆

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