octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]

Base Information

Chemical Name:octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]
CAS No.:1620164-68-2
Molecular Formula:C₂₄H₅₄N₂O₁₂P₄
Molecular Weight:686.594
Hs Code.:

Synonyms:octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]

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Chemical Property of octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]

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Technology Process of octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]

There total 4 articles about octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-1,4-diisocyanocyclohexane

: 122-52-1
triethyl phosphite

: 1620164-68-2
octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at -15 ℃; for 1h;
DOI:10.1016/j.bmcl.2014.05.071

Reference yield:

: 2615-25-0
trans-1,4-cyclohexyldiamine

: 122-51-0
orthoformic acid triethyl ester

: 762-04-9
phosphonic acid diethyl ester

: 1620164-68-2
octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]

Guidance literature:: at 125 ℃; for 15h;
DOI:10.3390/molecules25061424

Reference yield:

: 2615-25-0
trans-1,4-cyclohexyldiamine

: 1620164-68-2
octaethyl trans-cyclohexane-1,4-diylbis[aminomethylidene(bisphosphonate)]

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 8 h / Reflux

2.1: triethylamine / dichloromethane / 0 °C

2.2: 3 h / 0 - 20 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / -15 °C

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2014.05.071