5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile

Base Information

Chemical Name:5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile
CAS No.:886594-59-8
Molecular Formula:C₂₂H₂₀N₄O₃
Molecular Weight:388.426
Hs Code.:

5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1<i>H</i>-imidazol-4-yloxy]-isophthalonitrile

Synonyms:5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile

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Chemical Property of 5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile

Chemical Property:

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Technology Process of 5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile

There total 3 articles about 5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 453565-55-4
5-fluorobenzene-1,3-dicarbonitrile

: 1-(2,4-dimethoxy-benzyl)-5-ethyl-1,5-dihydro-imidazol-4-one

: 886594-59-8
5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 100 ℃; for 4h;
DOI:10.1021/ol060316x

Reference yield:

: 886594-58-7
2-(2,4-dimethoxy-benzylamino)-butyramide

: 886594-59-8
5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 2 h / 150 °C

2: 1.9 g / potassium carbonate / dimethylsulfoxide / 4 h / 100 °C

With potassium carbonate; acetic acid; In dimethyl sulfoxide;
DOI:10.1021/ol060316x

Reference yield:

: 20781-21-9
2,4-dimethoxybenzylamine hydrochloride

: 886594-59-8
5-[1-(2,4-dimethoxy-benzyl)-5-ethyl-1H-imidazol-4-yloxy]-isophthalonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / triethylamine / tetrahydrofuran / 72 h / 105 °C

2: acetic acid / 2 h / 150 °C

3: 1.9 g / potassium carbonate / dimethylsulfoxide / 4 h / 100 °C

With potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ol060316x