C₃₁H₃₅N₂O₉P

Base Information

Chemical Name:C₃₁H₃₅N₂O₉P
CAS No.:1554346-31-4
Molecular Formula:C₃₁H₃₅N₂O₉P
Molecular Weight:610.601
Hs Code.:

C<sub>31</sub>H<sub>35</sub>N<sub>2</sub>O<sub>9</sub>P

Synonyms:C₃₁H₃₅N₂O₉P

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Chemical Property of C₃₁H₃₅N₂O₉P

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Technology Process of C₃₁H₃₅N₂O₉P

There total 5 articles about C₃₁H₃₅N₂O₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1554346-34-7
C₂₂H₂₆NO₈P

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 1554346-31-4
C₃₁H₃₅N₂O₉P

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 5h;
DOI:10.1016/j.bmc.2013.12.034

Reference yield:

: C₁₉H₂₂NO₆P

: 1554346-31-4
C₃₁H₃₅N₂O₉P

Guidance literature:: Multi-step reaction with 3 steps

1: N,O-bis-(trimethylsilyl)-acetamide / dichloromethane / 22 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 7 h / 0 - 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 0 - 20 °C

With N,O-bis-(trimethylsilyl)-acetamide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2013.12.034

Reference yield:

: 130096-70-7
L-2-<<(benzyloxy)carbonyl>amino>-3-butenoic acid benzyl ester

: 1554346-31-4
C₃₁H₃₅N₂O₉P

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium hypophosphite; triethyl borane; oxygen / methanol; tetrahydrofuran / 5 h / 20 °C

2: N,O-bis-(trimethylsilyl)-acetamide / dichloromethane / 22 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 7 h / 0 - 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 0 - 20 °C

With N,O-bis-(trimethylsilyl)-acetamide; ammonium hypophosphite; triethyl borane; oxygen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmc.2013.12.034