C₁₂H₇Cl₂N₃

Base Information

Chemical Name:C₁₂H₇Cl₂N₃
CAS No.:845752-09-2
Molecular Formula:C₁₂H₇Cl₂N₃
Molecular Weight:264.114
Hs Code.:

C<sub>12</sub>H<sub>7</sub>Cl<sub>2</sub>N<sub>3</sub>

Synonyms:C₁₂H₇Cl₂N₃

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Chemical Property of C₁₂H₇Cl₂N₃

Chemical Property:

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Technology Process of C₁₂H₇Cl₂N₃

There total 10 articles about C₁₂H₇Cl₂N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: C₁₄H₉Cl₂N₃O

: 845752-09-2
C₁₂H₇Cl₂N₃

Guidance literature:: With lithium hydroxide; ethanol; water; at 79 ℃; for 3h;

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 845752-09-2
C₁₂H₇Cl₂N₃

Guidance literature:: Multi-step reaction with 10 steps

1: phosphorus pentachloride; trichlorophosphate / 5 h / 70 - 140 °C

2: dipotassium hydrogenphosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / DMF (N,N-dimethyl-formamide); water / 21 h / 68 °C

3: hydrogenchloride; iron / ethanol; water / 2 h / 90 °C

4: bromine; acetic acid / 23 h / 20 °C

5: methanesulfonic acid / 130 °C

6: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

7: pyrrolidine / ethanol / 0.25 h

8: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 2.5 h / 93 °C

9: potassium acetate; acetic anhydride / 14.5 h / 79 °C

10: lithium hydroxide; ethanol; water / 3 h / 79 °C

With pyrrolidine; hydrogenchloride; lithium hydroxide; dipotassium hydrogenphosphate; methanesulfonic acid; ethanol; phosphorus pentachloride; water; hydrogen; bromine; potassium acetate; acetic anhydride; iron; potassium carbonate; acetic acid; trichlorophosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); ethanol; water;

Reference yield:

: 845752-03-6
C₁₁H₈Cl₂N₂

: 845752-09-2
C₁₂H₇Cl₂N₃

Guidance literature:: Multi-step reaction with 7 steps

1: bromine; acetic acid / 23 h / 20 °C

2: methanesulfonic acid / 130 °C

3: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

4: pyrrolidine / ethanol / 0.25 h

5: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 2.5 h / 93 °C

6: potassium acetate; acetic anhydride / 14.5 h / 79 °C

7: lithium hydroxide; ethanol; water / 3 h / 79 °C

With pyrrolidine; lithium hydroxide; methanesulfonic acid; ethanol; water; hydrogen; bromine; potassium acetate; acetic anhydride; potassium carbonate; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water;