10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

Base Information

Chemical Name:10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine
CAS No.:168078-68-0
Molecular Formula:C₂₀H₁₇N₃O₃
Molecular Weight:347.373
Hs Code.:

Synonyms:10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

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Chemical Property of 10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

Chemical Property:

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Technology Process of 10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

There total 5 articles about 10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3113-71-1
3-methyl-4-nitrobenzoic acid

: 22162-53-4
10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine

: 168078-68-0
10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

Guidance literature:: With thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; chloroform;

Reference yield:

: 3958-60-9
2-nitrophenylmethyl bromide

: 168078-68-0
10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil

2: hydrogen / palladium-carbon / ethanol

3: thionyl chloride; N-ethyl-N,N-diisopropylamine / chloroform; dichloromethane

With sodium hydride; thionyl chloride; hydrogen; N-ethyl-N,N-diisopropylamine; palladium-carbon; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 22162-51-2
1-(2-Nitrobenzyl)-2-pyrrolecarboxaldehyde

: 168078-68-0
10,11-dihydro-10-(3-methyl-4-nitro-benzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium-carbon / ethanol

2: thionyl chloride; N-ethyl-N,N-diisopropylamine / chloroform; dichloromethane

With thionyl chloride; hydrogen; N-ethyl-N,N-diisopropylamine; palladium-carbon; In ethanol; dichloromethane; chloroform;