[4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester

Base Information

Chemical Name:[4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester
CAS No.:99668-25-4
Molecular Formula:C₁₃H₂₀ClO₂PS
Molecular Weight:306.793
Hs Code.:

Synonyms:[4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester

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Chemical Property of [4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester

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Technology Process of [4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester

There total 2 articles about [4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 115927-83-8
p-(diethylthiophosphono)cumyl alcohol

: 99668-25-4
[4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester

Guidance literature:: With thionyl chloride; for 0.333333h; Ambient temperature;
DOI:10.1021/jo00351a002

Reference yield:

: 60514-82-1
2-(4-iodophenyl)propan-2-ol

: 99668-25-4
[4-(1-Chloro-1-methyl-ethyl)-phenyl]-phosphonothioic acid O,O-diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / 5.5 h / Irradiation

2: 100 percent / thionyl chloride / 0.33 h / Ambient temperature

With thionyl chloride;
DOI:10.1021/jo00351a002