N,N'-bis(tert-butoxycarbonyl)-N,N₀-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene

Base Information

• Chemical Name: N,N'-bis(tert-butoxycarbonyl)-N,N₀-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene
• CAS No.: 1155245-01-4
• Molecular Formula: C₂₈H₄₀N₄O₆
• Molecular Weight: 528.649

Synonyms:N,N'-bis(tert-butoxycarbonyl)-N,N₀-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene

Chemical Property of N,N'-bis(tert-butoxycarbonyl)-N,N₀-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene

Chemical Property:

Purity/Quality:

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Technology Process of N,N'-bis(tert-butoxycarbonyl)-N,N₀-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene

There total 1 articles about N,N'-bis(tert-butoxycarbonyl)-N,N₀-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N,N'-bis(tert-butoxycarbonyl)-N,N'-bis[2-(tert-butyldiphenylsilyloxy)ethyl]-4,4'-aminomethylazobenzene (1155244-98-6) → N,N'-bis(tert-butoxycarbonyl)-N,N0-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene (1155245-01-4)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmc.2009.01.053

Reference yield:

di(succinimido) carbonate (74124-79-1) + N,N'-bis(tert-butoxycarbonyl)-N,N0-bis(2-hydroxyethyl)-4,4'-aminomethylazobenzene (1155245-01-4) → C38H46N6O14 (1155245-04-7)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.bmc.2009.01.053

upstream raw materials:

N,N'-bis(tert-butoxycarbonyl)-N,N'-bis[2-(tert-butyldiphenylsilyloxy)ethyl]-4,4'-aminomethylazobenzene

Downstream raw materials:

C₃₈H₄₆N₆O₁₄

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