4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure

Base Information

• Chemical Name: 4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure
• CAS No.: 153939-85-6
• Molecular Formula: C₁₈H₁₅FN₂O₂
• Molecular Weight: 310.328

Synonyms:4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure

Chemical Property of 4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure

Chemical Property:

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Technology Process of 4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure

There total 1 articles about 4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.4%

3-<2-Amino-1-(4-fluorphenyl)-ethyl>-indol Hydrochlorid + Glyoxilic acid (298-12-4) → 4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure (153939-85-6)

Guidance literature:

With sodium hydroxide; In water; for 14h; Ambient temperature; pH = 4;

DOI:10.1002/ardp.19933261009

Reference yield: 67.5%

4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure (153939-85-6) → 4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol Hydrochlorid

Guidance literature:

With hydrogenchloride; In water; for 2.5h; Heating;

DOI:10.1002/ardp.19933261009

Reference yield:

4-(4-Fluorphenyl)-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-carbonsaeure (153939-85-6) → 4-(4-Fluorphenyl)-2-phenylmethyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

Guidance literature:

Multi-step reaction with 2 steps

1: 67.5 percent / conc. HCl / H₂O / 2.5 h / Heating

2: 50.6 percent / 1.) conc.NH₃; 2.) Na₂CO₃ / ethanol / 60 h / Ambient temperature

With hydrogenchloride; ammonium hydroxide; sodium carbonate; In ethanol; water;

DOI:10.1002/ardp.19933261009

upstream raw materials:

Glyoxilic acid

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