1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene

Base Information

• Chemical Name: 1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene
• CAS No.: 1567359-93-6
• Molecular Formula: C₂₂H₃₆O₂Si
• Molecular Weight: 360.612
• Mol file: 1567359-93-6.mol

Synonyms:1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene

Chemical Property of 1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene

There total 1 articles about 1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-methylprop-1-en-1-yl)-1,3-dithiane (19860-69-6) + C17H28O3Si (345647-25-8) → 1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene (1567359-93-6) + 1-(4-methoxyphenyl)-4-methyl-1-(triisopropylsiloxy)-1,3-pentadiene (1567359-94-7)

Guidance literature:

With titanocene(II) triethylphosphite complex; In tetrahydrofuran; at 50 ℃; for 14h; Overall yield = 83 %; regioselective reaction;

DOI:10.1016/j.tetlet.2014.01.040

upstream raw materials:

2-(2-methylprop-1-en-1-yl)-1,3-dithiane

C₁₇H₂₈O₃Si