(1-azulenyl)diphenylsulfonium trifluoroacetate

Base Information

• Chemical Name: (1-azulenyl)diphenylsulfonium trifluoroacetate
• CAS No.: 1029874-04-1
• Molecular Formula: C₂F₃O₂*C₂₂H₁₇S
• Molecular Weight: 426.459
• Mol file: 1029874-04-1.mol

Synonyms:(1-azulenyl)diphenylsulfonium trifluoroacetate

Chemical Property of (1-azulenyl)diphenylsulfonium trifluoroacetate

Chemical Property:

Purity/Quality:

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Technology Process of (1-azulenyl)diphenylsulfonium trifluoroacetate

There total 1 articles about (1-azulenyl)diphenylsulfonium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,1'-sulfinylbisbenzene (945-51-7) + trifluoroacetic anhydride (407-25-0) + azulene (275-51-4) → (1-azulenyl)diphenylsulfonium trifluoroacetate (1029874-04-1)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/ejoc.200700959

Reference yield: 24.0%

(1-azulenyl)diphenylsulfonium trifluoroacetate (1029874-04-1) → azulen-1-yl(phenyl)sulfane (2978-89-4)

Guidance literature:

With diethylamine; In ethanol; for 0.5h; Reflux;

DOI:10.1002/ejoc.200700959

upstream raw materials:

1,1'-sulfinylbisbenzene

trifluoroacetic anhydride

azulene

Downstream raw materials:

azulen-1-yl(phenyl)sulfane