2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

Base Information

Chemical Name:2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran
CAS No.:96150-93-5
Molecular Formula:C₂₂H₃₂O₆
Molecular Weight:392.492
Hs Code.:

Synonyms:2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

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Chemical Property of 2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

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Technology Process of 2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

There total 3 articles about 2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2(S)-ethyl-2-<5(S)-(<2-(trimethylsilyl)ethoxymethoxy>methyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

: 96150-93-5
2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

Guidance literature:: With cesium fluoride; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 125 ℃; for 27h;
DOI:10.1021/ja00297a038

Reference yield:

: 2(S)-ethyl-2-<5(S)-carboxy-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran, methyl ester

: 96150-93-5
2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃;
DOI:10.1021/ja00297a038

Reference yield:

: 96150-95-7
2(S)-ethyl-2-<5(S)-carboxy-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

: 96150-93-5
2(S)-ethyl-2-<5(S)-(hydroxymethyl)-3(S)-methyl-2(R)-tetrahydrofuryl>-3(R),4(S)-(dimethylmethylenedioxy)-5(S)-(benzyloxy)tetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/ja00297a038