methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Base Information

Chemical Name:methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate
CAS No.:1604809-58-6
Molecular Formula:C₂₀H₂₂N₄O₃
Molecular Weight:366.42
Hs Code.:

Synonyms:methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

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Chemical Property of methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

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Technology Process of methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

There total 7 articles about methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylbenzenemethanamine

: 79-22-1
methyl chloroformate

: 1604809-58-6
methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 3h; Cooling with ice;

Reference yield:

: 40180-80-1
3-bromo-4-methylacetophenone

: 1604809-58-6
methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: N,N-dimethyl-formamide / 7 h / Inert atmosphere; Reflux

2: 16 h / 110 °C

3: hydrazine hydrate / ethanol / 1 h / Reflux

4: copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; sodium iodide / N,N-dimethyl-formamide / 96 h / 100 °C / Inert atmosphere

5: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 18 °C / Cooling with ice

6: potassium carbonate / tetrahydrofuran / 3 h / 20 °C / Cooling with ice

With copper(l) iodide; lithium aluminium tetrahydride; hydrazine hydrate; potassium carbonate; sodium iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 40180-77-6
5-acetyl-2-methylbenzonitrile

: 1604809-58-6
methyl N-[[5-[1-(6-methoxy-2-methyl-3-pyridinyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / toluene / Reflux

2: hydrazine hydrate / methanol / 2 h / Reflux

3: copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; sodium iodide / N,N-dimethyl-formamide / 96 h / 100 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 18 °C / Cooling with ice

5: potassium carbonate / tetrahydrofuran / 3 h / 20 °C / Cooling with ice

With copper(l) iodide; lithium aluminium tetrahydride; hydrazine hydrate; potassium carbonate; toluene-4-sulfonic acid; sodium iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;