succinyl bis

Base Information

Chemical Name:succinyl bis
CAS No.:147984-96-1
Molecular Formula:C₂₂H₂₄N₂O₆
Molecular Weight:412.442
Hs Code.:

Synonyms:succinyl bis

Suppliers and Price of succinyl bis

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of succinyl bis

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of succinyl bis

There total 2 articles about succinyl bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 147984-94-9
succinyl-Gly-OBzl

: 147984-96-1
succinyl bis

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; 1.) 0 deg C, 2 h, 2.) RT, overnight;
DOI:10.1246/bcsj.66.196

Reference yield:

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 147984-96-1
succinyl bis

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Et₃N / dimethylformamide / 1.) 0 deg C, 2 h, 2.) RT, overnight

2: 72 percent / Et₃N, HOBt, DCC / CH₂Cl₂ / 1.) 0 deg C, 2 h, 2.) RT, overnight

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.66.196

Reference yield:

: 147984-96-1
succinyl bis

: 147984-98-3
succinyl bis

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / H₂ / Pd / dimethylformamide / 5 h

2: 81 percent / Et₃N, HOBt, EDC*HCl / dimethylformamide / 1.) 0 deg C, 2 h, 2.) RT, overnight

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium; In N,N-dimethyl-formamide;
DOI:10.1246/bcsj.66.196