1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide}

Base Information

• Chemical Name: 1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide}
• CAS No.: 1207158-52-8
• Molecular Formula: C₃₁H₄₀N₂O₂Si
• Molecular Weight: 500.756

Synonyms:1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide}

Chemical Property of 1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide}

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide}

There total 1 articles about 1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,1,3,3-tetramethylisoindoline-[N-(4-bromophenyl)-5,6-dicarboximide] (1207158-50-6) + tris-iso-propylsilyl acetylene (89343-06-6) → 1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide} (1207158-52-8)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triethylamine; tris-(o-tolyl)phosphine; In toluene; at 50 ℃; for 40h; Inert atmosphere;

DOI:10.1002/chem.200902162

Reference yield: 90.0%

1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide} (1207158-52-8) → 1,1,3,3-tetramethyl-2-oxylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide} (1207158-54-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1002/chem.200902162

Reference yield: 85.0%

1,1,3,3-tetramethylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide} (1207158-52-8) → 1,1,3,3-tetramethylisoindoline-[N-(4-ethynylphenyl)-5,6-dicarboximide] (1207158-53-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃;

DOI:10.1002/chem.200902162

upstream raw materials:

1,1,3,3-tetramethylisoindoline-[N-(4-bromophenyl)-5,6-dicarboximide]

tris-iso-propylsilyl acetylene

Downstream raw materials:

1,1,3,3-tetramethylisoindoline-[N-(4-ethynylphenyl)-5,6-dicarboximide]

1,1,3,3-tetramethyl-2-oxylisoindoline-{N-[4-(triisopropylsilylethynyl)phenyl]-5,6-dicarboximide}

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