Technology Process of C17H16O2
There total 3 articles about C17H16O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
18-crown-6 ether; potassium peroxomonosulfate; sodium hydrogencarbonate; acetone;
In
water; acetonitrile;
at 0 ℃;
Inert atmosphere;
DOI:10.1039/c2cc17960a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere
2: potassium peroxomonosulfate; 18-crown-6 ether; sodium hydrogencarbonate; acetone / water; acetonitrile / 0 °C / Inert atmosphere
With
18-crown-6 ether; potassium peroxomonosulfate; sodium hydrogencarbonate; acetone; pyridinium chlorochromate;
In
dichloromethane; water; acetonitrile;
DOI:10.1039/c2cc17960a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere
4.1: potassium peroxomonosulfate; 18-crown-6 ether; sodium hydrogencarbonate; acetone / water; acetonitrile / 0 °C / Inert atmosphere
With
n-butyllithium; 18-crown-6 ether; potassium peroxomonosulfate; sodium hydrogencarbonate; acetone; pyridinium chlorochromate;
In
tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1039/c2cc17960a