Technology Process of C34H42O3Si
There total 7 articles about C34H42O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Grubbs catalyst first generation;
In
dichloromethane;
at 43 ℃;
for 12h;
Overall yield = 84 %; Overall yield = 84 mg;
DOI:10.1021/ol500667d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
2.1: copper(l) chloride; hydroxylamine hydrochloride; N-butylamine / dichloromethane; water / 0.5 h / 0 - 20 °C / Inert atmosphere
2.2: 0.5 h / 0 - 20 °C / Inert atmosphere
3.1: Grubbs catalyst first generation / dichloromethane / 12 h / 43 °C
With
Grubbs catalyst first generation; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; N-butylamine; copper(l) chloride;
In
tetrahydrofuran; dichloromethane; water;
2.1: |Cadiot-Chodkiewicz Coupling / 2.2: |Cadiot-Chodkiewicz Coupling;
DOI:10.1021/ol500667d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper(l) chloride; hydroxylamine hydrochloride; N-butylamine / dichloromethane; water / 0.5 h / 0 - 20 °C / Inert atmosphere
1.2: 0.5 h / 0 - 20 °C / Inert atmosphere
2.1: Grubbs catalyst first generation / dichloromethane / 12 h / 43 °C
With
Grubbs catalyst first generation; hydroxylamine hydrochloride; N-butylamine; copper(l) chloride;
In
dichloromethane; water;
1.1: |Cadiot-Chodkiewicz Coupling / 1.2: |Cadiot-Chodkiewicz Coupling;
DOI:10.1021/ol500667d
