Technology Process of C2HF3O2*C37H41N5O6S
There total 8 articles about C2HF3O2*C37H41N5O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H32N2O7S; 4-(aminomethyl)benzene-1-carboximidamide dihydrochloride;
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
trifluoroacetic acid;
In
acetonitrile;
DOI:10.1021/jm2011996
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride; acetic acid / 1 h / 20 °C
2: sodium hydroxide / water; acetonitrile / 4.5 h / pH 7 - 8
3: water; sodium hydroxide / 1,4-dioxane / 1 h / 40 °C
4: palladium 10% on activated carbon; ethyl acetate / 3 h / 20 °C
5: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
With
hydrogenchloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; acetic acid; ethyl acetate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm2011996
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; sodium hydroxide / 1,4-dioxane / 1 h / 40 °C
2: palladium 10% on activated carbon; ethyl acetate / 3 h / 20 °C
3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
With
palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; ethyl acetate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm2011996
