2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside
CAS No.:103614-84-2
Molecular Formula:C₂₀H₂₃ClN₂O₁₁
Molecular Weight:502.862
Hs Code.:

Synonyms:2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

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Technology Process of 2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

There total 1 articles about 2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.5%

: 619-08-9
2-chloro-4-nitrophenol

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 103614-84-2
2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With triethylamine; In acetonitrile; at 40 ℃; for 2h;
DOI:10.1248/cpb.43.266

Reference yield: 73.8%

: 103614-84-2
2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 163729-58-6
4-amino-2-chlorophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane; for 6h; under 760 Torr; Ambient temperature;
DOI:10.1248/cpb.43.266

Reference yield:

: 103614-84-2
2-chloro-4-nitrophenyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 4-amino-2-chlorophenyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 73.8 percent / H₂ / 10percent Pd/C / dioxane / 6 h / 760 Torr / Ambient temperature

2: 85.9 percent / 28percent NaOMe / methanol; acetonitrile; CHCl₃ / 1 h / Ambient temperature

With hydrogen; sodium methylate; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform; acetonitrile;
DOI:10.1248/cpb.43.266