(5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one

Base Information

Chemical Name:(5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one
CAS No.:521916-68-7
Molecular Formula:C₂₄H₂₉NO₅
Molecular Weight:411.498
Hs Code.:

Synonyms:(5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one

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Chemical Property of (5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one

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Technology Process of (5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one

There total 9 articles about (5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 521916-67-6
Thiocarbonic acid O-((2R,5R,6R,7R,7aR)-6-benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-3-oxo-hexahydro-pyrrolizin-2-yl) ester O-phenyl ester

: 521916-68-7
(5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;

Reference yield:

: 521916-74-5
(2R,3R,4R)-3-Benzyloxy-2-benzyloxymethyl-4-methoxymethoxy-3,4-dihydro-2H-pyrrole 1-oxide

: 521916-68-7
(5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 31 percent / benzene / 15 h / 20 °C

2: Zn; aq. AcOH / 90 °C

3: pyridine; DMAP / CH₂Cl₂

4: Bu₃SnH; AIBN / benzene / Heating

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; acetic acid; zinc; In dichloromethane; benzene;

Reference yield:

: C₃₇H₄₅NO₆Si

: 521916-68-7
(5R,6R,7R,7aR)-6-Benzyloxy-5-benzyloxymethyl-7-methoxymethoxy-hexahydro-pyrrolizin-3-one

Guidance literature:: Multi-step reaction with 6 steps

1: Et₃N / toluene / 0 °C

2: 72 percent / Bu₄N(+)Ph₃SiF₂(-); 4 Angstroem molecular sieves / tetrahydrofuran / 0.25 h / Heating

3: 31 percent / benzene / 15 h / 20 °C

4: Zn; aq. AcOH / 90 °C

5: pyridine; DMAP / CH₂Cl₂

6: Bu₃SnH; AIBN / benzene / Heating

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tri-n-butyl-tin hydride; acetic acid; triethylamine; tetrabutylammonium triphenyldifluorosilicate; zinc; In tetrahydrofuran; dichloromethane; toluene; benzene;